Publications: 2006 – 2010

2010
S. Marre, A. Adamo, Soubir Basak, Cyril Aymonier and K.F. Jensen, “Design and packaging of microreactors for high pressure and high temperature applications,” Ind. Eng.Chem. Res. http://dx.doi.org/10.1021/ie101346u

W. Chan, P. Bermel, R. Pilawa, C. Marton, K.F. Jensen, M. Soljacic, J. Joannopoulos, and I. Celanovic, “A high-efficiency millimeter-scale thermophotovoltaic generator thermo photovoltaic generation of electricity”, European Photovoltaic Solar Energy Conference 25th EU PVSEC) / 5th World Conference on Photovoltaic Energy Conversion (WCPEC-5) 6 – 9 September 2010, Valencia, Spain. 461_Chan_eupvsec25_10.pdf

P. Bermel, M. Ghebrebrhan, W. Chan, Y.X. Yeng, M. Araghchini, R. Hamam, C.H. Marton, K.F. Jensen, M. Soljačić, J.D. Joannopoulos, S.G. Johnson, and I. Celanovic, “Design and global optimization of high-efficiency thermophotovoltaic systems,” Optics Express. 18(S3) A314-A334 (2010) 459_Bermel_OE_2010.pdf

J.P. McMullen and K.F. Jensen, “An automated microfluidic system for online optimization in chemical synthesis,” Org. Process Res. Dev., 14, 1169–1176 (2010) http://dx.doi.org/10.1021/op100123e

J.P. McMullen, M.T. Stone, S.L. Buchwald, and K.F. Jensen, “An integrated microreactor system for self-optimization of a heck reaction: From micro- to mesoscale flow systems,” Angew Chemie Int. Ed., 49 (39) 7076–7080 (2010) http://dx.doi.org/10.1002/anie.201002590

R.L. Hartman, J.R. Naber, N. Zaborenko, S.L. Buchwald, and K.F. Jensen, “Overcoming the challenges of solid bridging and constriction during Pd-catalyzed C-N bond formation in microreactors,” Org. Process Res. Dev., http://dx.doi.org/10.1021/op100154d

S. Marre, A. Adamo, Soubir Basak, Cyril Aymonier and K.F. Jensen, “Design and packaging of microreactors for high pressure and high temperature applications,” Ind. Eng.Chem. Res. http://dx.doi.org/10.1021/ie101346u

N. Zaborenko, E.R. Murphy, J.G. Kralj, and K. F. Jensen, “Synthesis and Kinetics of Highly Energetic Intermediates by Micromixers: Direct Multistep Synthesis of Sodium Nitrotetrazolate, “Ind. Eng.Chem. Res. 49 (9) 4132–4139 (2010) http://dx.doi.org/10.1021/ie100263p

K. Deshpande, J.H. Meldon, M. A. Schmidt, and K.F. Jense, “SOI supported microdevice for hydrogen purification using palladium-silver membranes,” J. Microelectromechanical Systems 19 (2) 402 – 409 (2010) http://dx.doi.org/10.1109/JMEMS.2010.2041529

J. Wen, J. Albrecht, and K.F. Jensen, “Microfluidic preparative free-flow isoelectric focusing in a triangular channel: System development and characterization,” Electrophoresis 31, 1606–1614 (2010) http://dx.doi.org/10.1002/elps.200900577

S. Marre and K.F. Jensen,”Synthesis of nanostructures in microfluidic systems,” Chem. Soc. Rev. (RSC), 39, 1183 – 1202 (2010) http://dx.doi.org/10.1039/b821324k

J. Wen, E.W. Wilker, M.B. Yaffe, and K.F. Jensen,”Microfluidic preparative free-flow isoelectric focusing: System optimization for protein complex separation,” Anal. Chem. 82 (4) 1253–1260 (2010) http://dx.doi.org/10.1021/ac902157e

M.W. Bedore, N. Zaborenko, K.F. Jensen, and T.F. Jamison, “Aminolysis of exides in a microreactor system: A continuous flow approach to β-amino alcohols,” Org. Proc. Res. Dev. Org. Proc. Res. Dev., 14, 432–440 (2010) http://dx.doi.org/10.1021/op9003136

J.P. McMullen and K.F. Jensen, “Integrated microreactors for reaction automation: New approaches to reaction development,” Annu. Rev. Anal. Chem. 3 19–42 (2010) http://dx.doi.org/10.1146/annurev.anchem.111808.073718

R. L. Hartman, J. R. Naber, S. L. Buchwald, and K. F. Jensen, “Multistep microchemical synthesis enabled by microfluidic distillation,” Angew Chemie Int. Ed. 49 899-903 (2010) http://dx.doi.org/10.1002/anie.200904634

S. Marre, J. Baek, J. Park, M. G. Bawendi, K. F. Jensen, “High-pressure/high-temperature microreactors for nanostructure synthesis,” J. Association for Laboratory Automation 14 (6) 367-373, http://dx.doi.org/10.1016/j.jala.2009.06.005

L. Chao, A.P. Gast, T.A. Hatton, and K.F. Jensen “Sphingomyelinase-induced phase transformations: causing morphology switches and multiple-time-domain ceramide generation in model raft membranes,” Langmuir 26(1), 344–356 (2010) http://dx.doi.org/10.1021/la902084u

2009
R. Hartman and K.F. Jensen,“Microchemical systems for continuous-flow synthesis,“ Lab Chip, 9, 2495 – 2507 (2009) http://dx.doi.org/10.1039/b906343a

J.R. Goodell, J.P. McMullen,N. Zaborenko, J.R. Maloney, C-X. Ho, K.F. Jensen, J.A. Porco Jr., and A.B. Beeler, “Development of an automated microfluidic reaction platform for multidimensional screening: reaction discovery employing bicyclo[3.2.1]octanoid scaffolds,” J. Org. Chem. 74 (16) 6169–6180 (2009) http://dx.doi.org/10.1021/jo901073v

N. de Mas, A. Günther,| M.A. Schmidt, and K. F. Jensen, ”Increasing productivity of microreactors for fast gas-liquid reactions: The case of direct fluorination of toluene,” Ind. Eng. Chem. Res. 48 (3) 1428–1434 (2009) http://dx.doi.org/10.1021/ie801232d

R. Hartman and K.F. Jensen,“ Distillation in microchemical systems by using capillary forces and segmented flow,“ Lab Chip, 9, 1843 – 1849 (2009) http://dx.doi.org/10.1039/b901790a

J.Y. Rempel, M.G. Bawendi, and K.F. Jensen,”Insights into the kinetics of semiconductor nanocrystal nucleation and growth,” J. Am. Chem. Soc. 131 (12) 479–4489 (2009) http://dx.doi.org/10.1021/ja809156t

2008
S. Marre, J. Park, J. Rempel, J. Guan, M.G. Bawendi, and K.F. Jensen,”Supercritical continuous-microflow synthesis of narrow size distribution quantum dots,” Adv. Mater. 20, 4830–4834 (2008) http://dx.doi.org/10.1002/adma.200801579

J.P McMullen and KF Jensen, “An intelligent microreactor system for real-time optimization of a chemical reaction,” Proceedings of the 12th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2008) (Eds. L.E. Locascio, M. Gaitan, B.M. Paegel, D.J. Ross, W.N. Vreeland) pp. 1107-9. 440_McMullen_mTAS.pdf

J. Wen, J. Albrecht, E. W. Wilker, M. B. Yaffe and K.F. Jensen, “Microfluidic Protein separation by free flow isoelectric focusing,” Proceedings of the 12th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2008) (Eds. L.E. Locascio, M. Gaitan, B.M. Paegel, D.J. Ross, W.N. Vreeland) pp. 492-4. 439_Wen_mTAS.pdf

B.A. Wilhite, T.F. Hill, L. F. Velasquez-Garcia, A.H. Epstein, K.F. Jensen, and C. Livermore, “Design of a silicon-based microscale trickle-bed system for singlet-oxygen production,” AIChE Journal, 54 ( 9) 2441-2455 (2008) http://dx.doi.org/10.1002/aic.11564

Adamo and K.F. Jensen, “Microfluidic based single cell microinjection,” Lab Chip, 8, 1258–1261 (2008) http://dx.doi.org/10.1039/b803212b

M. Kreutzer, A.Günther, and K.F. Jensen, “Sample dispersion in segmented flow through microchannels with rectangular cross section,” Anal. Chem. 80, 1558-1567 (2008) http://dx.doi.org/10.1021/ac702143r

2007
J. W. Albrecht, J. El-Ali, and K. F. Jensen, “Cascaded free-flow isoelectric focusing for improved focusing speed and resolution,” Anal. Chem. 79 9364-9371 (2007) http://dx.doi.org/10.1021/ac071574q

L. Ye, M. Zhang, L.G. Alexopoulos, P.K. Sorger, and K.F. Jensen, ”Microfluidic devices for studying the response of adherent cells under short time stimuli treatment,” Proceedings of the 11th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2007), J.L. Viovy, P. Tabeling. (Eds.) October 7-11, 2007, Paris, France pp. 152-153. 434_Ye_mTAS_07.pdf

S. A. Khan and K. F. Jensen, “Oscillatory bubbling in a microfluidic T-junction,” Proceedings of the 11th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2007), J.L. Viovy, P. Tabeling. (Eds.) October 7-11, 2007, Paris, France, pp. 952-3. 434b_Khan_mTAS_07.pdf

T F. Hill, L.F. Velásquez-García, B.A. Wilhite, W.T. Rawlins, S. Lee, K.F. Jensen, A.H. Epstein, and C. Livermore, “A MEMS singlet oxygen generator – Part II: Experimental exploration of the performance space,” J. Microelectromechanical Systems 16 (6) 1492 – 1505 (2007) http://dx.doi.org/10.1109/JMEMS.2007.907880

L.F. Velásquez-García, T.F. Hill, B.A. Wilhite, K.F. Jensen, A.H. Epstein, and C. Livermore, “A MEMS singlet oxygen generator – Part I: Device fabrication and proof of concept demonstration,” J. Microelectromechanical Systems 16 (6) 1482 – 1491 (2007) http://dx.doi.org/10.1109/JMEMS.2007.902446

E. R. Murphy, T. Inoue, H.R. Sahoo, N. Zaborenko and Klavs F. Jensen, “Solder-based chip-to-tube and chip-to-chip packaging for microfluidic,” Lab Chip, 7, 1309–1314 (2007) http://dx.doi.org/10.1039/b704804a

D. J. Quiram, K. F. Jensen, M. A. Schmidt, P. L. Mills, J. F. Ryley, M. D. Wetzel, and D. J. Kraus, “Integrated microreactor system for gas-phase catalytic reactions. 3. Microreactor system design and system automation,” Ind. Eng. Chem. Res. 46 (25); 8319-8335 (2007) http://dx.doi.org/10.1021/ie0702577

D. J. Quiram, K. F. Jensen, M. A. Schmidt, P. L. Mills, J. F. Ryley, M. D. Wetzel, and D. J. Kraus, “Integrated microreactor system for gas-phase catalytic reactions. 2. Microreactor packaging and testing, ”Ind. Eng. Chem. Res. 46 (25), 8306 -8318 (2007) http://dx.doi.org/10.1021/ie070108o

D. J. Quiram, K. F. Jensen, M. A. Schmidt, P. L. Mills, J. F. Ryley, M. D. Wetzel, and D. J. Kraus, “Integrated microreactor system for gas-phase catalytic reactions. 1. Scale-up microreactor design and fabrication,” Ind. Eng. Chem. Res., 46 (25), 8292 -8305 (2007) http://dx.doi.org/10.1021/ie070107w

S.A. Khan and K.F. Jensen, “Microfluidic synthesis of titania shells on colloidal silica,” Adv. Mater. 19, 2556–2560 (2007) http://dx.doi.org/10.1002/adma.200700127

K.F. Jensen, “Microchemical Systems for Discovery and Development,” in “New Avenues to Efficient Chemical Synthesis – Emerging Technologies,” (P.H. Seeberger and T. Blume) Ernst Schering Foundation, Symposium Proceedings 06.3, Springer 2007 pp. 57-76, http://dx.doi.org/10.1007/b12018970-0004

H. R. Sahoo, J. G. Kralj and K. F. Jensen, “Multi-step continuous flow microchemical synthesis involving multiple reactions and separations,” Angew. Chemie Int. Ed. 46, 5704 –5708 (2007) http://dx.doi.org/10.1002/anie.200701434

L.R. Arana, N. de Mas, R. Schmidt, A.J. Franz, M.A. Schmidt, and K.F. Jensen, “Isotropic etching of silicon in fluorine gas for MEMS micromachining,” J. Micromech. Microeng. 17 384–392 (2007) http://dx.doi.org/10.1088/0960-1317/17/2/026

H.-G. Choi, J. P. Amara, T.P. Martin, K.K. Gleason, T.M. Swager, and K.F. Jensen, “Directed growth of poly(isobenzofuran) films by chemical vapor deposition on patterned self-assembled monolayers as templates,” Langmuir 23 2483-2491 (2007) http://dx.doi.org/10.1021/la062268v

T. Inoue, M.A. Schmidt, and K.F. Jensen, Microfabricated multiphase reactors for the direct synthesis of hydrogen peroxide from hydrogen and oxygen,” Ind. Eng. Chem. Res. 46, 1153-1160 (2007) http://dx.doi.org/10.1021/ie061277w

E.R. Murphy, J.R. Martinelli, N. Zaborenko, S.L. Buchwald and K.F. Jensen, “Accelerating reactions with microreactors at elevated temperature and pressures: profiling aminocarbonylation reactions”, Angew. Chemie Int. Ed.. 46, 1734-1737 (2007) http://dx.doi.org/10.1002/anie.200604175

Z. Zhang, G. Perozziello, P. Boccazzi, A.J. Sinskey, O. Geschke, and K.F. Jensen, “Microbioreactors for bioprocess development,” J. Association for Laboratory Automation, 12 (3) 143-151 (2007) http://dx.doi.org/10.1016/j.jala.2006.10.017

J.G. Kralj, H.R. Sahoo and K.F. Jensen, “Integrated continuous microfluidic liquid-liquid extraction,” Lab Chip, 7, 256 – 263 (2007) http://dx.doi.org/10.1039/b610888a

2006
G.-S. Kim, T. Merchant, J. D’Urso, L.A. Gochberg, and K.F. Jensen, “Systematic study of surface chemistry and comprehensive two-dimensional tertiary current distribution model for copper electrochemical deposition,” J. Electrochem. Soc., 153 (11) C761-C772 (2006) http://dx.doi.org/10.1149/1.2337767

H.-G. Choi, J. P. Amara, T.P. Martin, K.K. Gleason, T.M. Swager, and K.F. Jensen, “Structure and morphology of poly(isobenzofuran) films grown by hot-filament chemical vapor deposition,” Chem. Mater. 18, 6339-6344 (2006) http://dx.doi.org/10.1021/cm0616331

A. Adamo and K. F. Jensen, “Microfluidics for controlled single cell microinjection,” “Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp.1492-4. 417_Adamo_mTAS_06.pdf

J. El-Ali and K.F. Jensen, “Microcarrier enabled microfluidic assays of anchorage dependant cells,” “Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp.1486-8. 416_ElAli_mTAS_06.pdf

H.R. Sahoo, J.G. Kralj and K.F. Jensen, “Multi-step continuous microchemical synthesis and separation,” “Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp.1029-31. 415_Sahoo_mTAS_06.pdf

Z. Zhang, P. Boyle, R.Kolfschoten, P. Boccazzi, A.J. Sinskey, and K.F. Jensen, “Evaporation- and pressure- driven closedloop pH control in a microliter bioreactor for high-throughput bioprocessing,”“Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp.966-8. 414_Zhang_mTAS_06.pdf

J. Albrecht and K.F. Jensen, “Multi-stage free-flow isoelectric focusing for enhanced separation speed and resolution,” “Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp.921-3. 413_Albrect_mTAS_06.pdf

A. Günther and K.F. Jensen, “Multiphase microfluidics near the speed of sound,” “Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp. 537-9. 412_Gunther_mTAS_06.pdf

S. A. Khan, V. Gondoin and K.F. Jensen,”Integrated microreactor for continuous colloid synthesis and surface-coating,” in Proceedings of the 10th International Conference on Miniaturized Systems for Chemistry and Life Sciences (μTAS2006), T. Kitamori, H. Fujita, and S. Hasabe (Eds.) November 5-9, 2006, Tokyo, Japan, pp. 257-9. 411_Khan_06.pdf

Y. Wada, M.A. Schmidt, and K.F. Jensen, “Flow distribution and ozonolysis in gas-liquid multi-channel microreactors, Ind. Eng. Chem. Res. 45, 8036-8042 (2006) http://dx.doi.org/10.1021/ie060893p

J.W. Albrecht and K.F. Jensen, “Micro free flow isoelectric focusing enhanced by active cooling and functionalized gels,” Electrophoresis, 27, 4960–4969 (2006) http://dx.doi.org/10.1002/elps.200600436

A. Günther and K.F. Jensen,” Multiphase microfluidics: from flow characteristics to chemical and materials synthesis,” Lab. Chip., 6, 1487 – 1503 (2006) http://dx.doi.org/10.1039/b609851g

J.G. Kralj, M.T.W. Lis, M.A. Schmidt, and K.F. Jensen, “Continuous dielectrophoretic size-based particle sorting,” Analytical Chemistry, 78 5019-5025 (2006) http://dx.doi.org/10.1021/ac0601314

J.Y. Rempel, B.L. Trout, M.G. Bawendi, and K.F. Jensen, “Density functional theory study of ligand binding on CdSe (0001), (000), and (110) single crystal relaxed and reconstructed surfaces: Implications for nanocrystalline growth,” J. Phys. Chem. B 110 18007-18016 (2006) http://dx.doi.org/10.1021/jp064051f

H.-G. Choi, J.P. Amara, T.M. Swager, and K.F. Jensen,”Synthesis and characterization of poly(isobenzofuran) films by chemical vapor deposition,” Macromolecules, 39, 4400-4410 (2006) http://dx.doi.org/10.1021/ma060345n

J. El-Ali, P.K. Sorger, and K.F. Jensen, Cells on Chips. Nature 442, 403-411(2006) http://dx.doi.org/10.1038/nature05063

P. Boccazzi, Z. Zhang, Kazuhiko Kurosawa, N, Szita, Bhattacharya., K.F. Jensen, A.J. Sinskey, “Differential gene expression profiles and real-time measurements of growth parameters in Saccharomyces cerevisiae grown in microliter-scale bioreactors equipped with internal stirring,” Biotechnology Progress, 22;710-717 (2006) http://dx.doi.org/10.1021/bp0504288

T.F. Hill, L.F. Velásquez-García, B.A. Wilhite, K.F. Jensen, A.H. Epstein, and C. Livermore, “A MEMS singlet oxygen generator,” Technical Digest, Solid State Sensor and Actuator Workshop, Hilton Head, SC. June 2006. 401_Hill_06.pdf

Z. Zhang, P. Boccazzi, H.-G. Choi, G. Perozziello, A.J. Sinskey, and K.F. Jensen, “Microchemostat – microbial continuous culture in a polymer-based, instrumented microbioreactor, “Lab-on-a-Chip 6, 906–913 (2006) http://dx.doi.org/10.1039/b518396k

B.A. Wilhite, S.E. Weiss, J.Y. Ying, M.A. Schmidt, and K. F. Jensen, “High-purity hydrogen generation in a microfabricated 23 wt % Ag-Pd membrane device integrated with 8:1 LaNi0.95Co0.05O3 /Al2O3 Catalyst,” Adv. Mater. 18, 1701–1704 (2006). (Highlighted in News and Views perspective in Nature, R.I. Masel, “Hydrogen quick and clean,” Nature, 442, 521-2, (2006) http://dx.doi.org/10.1002/adma.200502025

T. Gervais, J. El-Ali, A. Guenther, and K. F. Jensen, “Flow-induced deformation of shallow microfluidic channels,” Lab-on-a-Chip 6, 500-507 (2006) http://dx.doi.org/10.1039/b513524a

W. Sheng, S. Kim, J. Lee, S.-W. Kim, K. F. Jensen, and M. G. Bawendi, “In-situ encapsulation of quantum dots into polymer microspheres,” Langmuir, 22, 3782-3790 (2006) http://dx.doi.org/10.1021/la051973l

K.F. Jensen, “Silicon based microchemical systems –Characteristics and applications,” Materials Research Society Bulletin 31, 101-107 (2006). 396_Jensen_06.pdf

Z. Zhang, N. Szita, P. Boccazzi, A. J. Sinskey, and K. F. Jensen, “ A well-mixed, polymer-based microbioreactor with integrated optical measurements,” Biotech. Bioeng. 93, 286-296 (2006) http://dx.doi.org/10.1002/bit.20678

T. Gervais and K.F. Jensen, “Mass transport and surface reactions in microfluidic systems,” Chem. Eng. Sci. 61 1102–1121 (2006) http://dx.doi.org/10.1016/j.ces.2005.06.024

Zanzotto, P. Boccazzi, N. Gorret, T.K. Van Dyk, A.J. Sinskey, and K.F. Jensen, “In situ measurement of bioluminescence and fluorescence in an integrated microbioreactor,” Biotech. Bioeng. 93 40-47 (2006) http://dx.doi.org/10.1002/bit.20708